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[Keyword] roughness(20hit)

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  • A Study on Substrate Orientation Dependence of Si Surface Flattening Process by Sacrificial Oxidation and Its Effect on MIS Diode Characteristics

    Sohya KUDOH  Shun-ichiro OHMI  

     
    PAPER

      Vol:
    E99-C No:5
      Page(s):
    504-509

    In this study, we investigated Si(100), Si(110) and Si(111) surface flattening process utilizing sacrificial oxidation method, and its effect on Metal-Insulator-Semiconductor (MIS) diode characteristics. By the etching of the 100 nm-thick sacrificial oxide formed by thermal oxidation at 1100°C, the surface roughness of Si(100), Si(110) and Si(111) substrates were reduced. The obtained Root-Mean-Square (RMS) roughness of Si(100) was reduced from 0.22 nm (as-cleaned) to 0.07 nm (after etching), while it was reduced from 0.23 nm to 0.12 nm in the case of Si(110), and from 0.23 nm to 0.11 nm in the case of Si(111), respectively. Furthermore, it was found that time-dependent dielectric breakdown (TDDB) characteristics of MIS diodes for p-Si(100), p-Si(110) and p-Si(111) were improved with the reduction of Si surface RMS roughness.

  • A Study on Si(100) Surface Flattening Utilizing Sacrificial Oxidation Process and Its Effect on MIS Diode Characteristics

    Sohya KUDOH  Shun-ichiro OHMI  

     
    PAPER

      Vol:
    E98-C No:5
      Page(s):
    402-405

    In this study, Si(100) surface flattening process was investigated utilizing sacrificial oxidation method to improve Metal--Insulator--Semiconductor (MIS) diode characteristics. By etching of the 100,nm-thick sacrificial oxide formed by thermal oxidation at 1100$^{circ}$C, the surface roughness of Si substrate was reduced. The obtained Root-Mean-Square (RMS) roughness was decreased from 0.15,nm (as-cleaned) to 0.07,nm in the case of sacrificial oxide formed by wet oxidation, while it was 0.10,nm in the case of dry oxidation. Furthermore, time-dependent dielectric breakdown (TDDB) characteristic of Al/SiO$_{2}$(10,nm)/p-Si(100) MIS diode structures was found to be improved by the reduction of Si surface RMS roughness.

  • Roughness Classification with Aggregated Discrete Fourier Transform

    Chao LIANG  Wenming YANG  Fei ZHOU  Qingmin LIAO  

     
    PAPER-Image Recognition, Computer Vision

      Vol:
    E97-D No:10
      Page(s):
    2769-2779

    In this paper, we propose a texture descriptor based on amplitude distribution and phase distribution of the discrete Fourier transform (DFT) of an image. One dimensional DFT is applied to all the rows and columns of an image. Histograms of the amplitudes and gradients of the phases between adjacent rows/columns are computed as the feature descriptor, which is called aggregated DFT (ADFT). ADFT can be easily combined with completed local binary pattern (CLBP). The combined feature captures both global and local information of the texture. ADFT is designed for isotropic textures and demonstrated to be effective for roughness classification of castings. Experimental results show that the amplitude part of ADFT is also discriminative in describing anisotropic textures and it can be used as a complementary descriptor of local texture descriptors such as CLBP.

  • Influence of Si Surface Roughness on Electrical Characteristics of MOSFET with HfON Gate Insulator Formed by ECR Plasma Sputtering

    Dae-Hee HAN  Shun-ichiro OHMI  Tomoyuki SUWA  Philippe GAUBERT  Tadahiro OHMI  

     
    PAPER

      Vol:
    E97-C No:5
      Page(s):
    413-418

    To improve metal oxide semiconductor field effect transistors (MOSFET) performance, flat interface between gate insulator and silicon (Si) should be realized. In this paper, the influence of Si surface roughness on electrical characteristics of MOSFET with hafnium oxynitride (HfON) gate insulator formed by electron cyclotron resonance (ECR) plasma sputtering was investigated for the first time. The surface roughness of Si substrate was reduced by Ar/4.9%H2 annealing utilizing conventional rapid thermal annealing (RTA) system. The obtained root-mean-square (RMS) roughness was 0.07nm (without annealed: 0.18nm). The HfON was formed by 2nm-thick HfN deposition followed by the Ar/O2 plasma oxidation. The electrical properties of HfON gate insulator were improved by reducing Si surface roughness. It was found that the current drivability of fabricated nMOSFETs was remarkably increased by reducing Si surface roughness. Furthermore, the reduction of Si surface roughness also leads to decrease of the 1/f noise.

  • Flattening Process of Si Surface below 1000 Utilizing Ar/4.9%H2 Annealing and Its Effect on Ultrathin HfON Gate Insulator Formation

    Dae-Hee HAN  Shun-ichiro OHMI  

     
    PAPER

      Vol:
    E96-C No:5
      Page(s):
    669-673

    To improve metal oxide semiconductor field effect transistors (MOSFET) performance, flat interface between gate insulator and silicon should be realized. In this paper, flattening process of Si surface below 1000 utilizing Ar/4.9%H2 annealing and its effect on ultrathin HfON gate insulator formation were investigated. The Si(100) substrates were annealed using conventional rapid thermal annealing (RTA) system in Ar or Ar/4.9%H2 ambient for 1 h. The surface roughness of Ar/4.9%H2-annealed Si was small compared to that of Ar-annealed Si because the surface oxidation was suppressed. The obtained root mean square (RMS) roughness was 0.08 nm (as-cleaned: 0.20 nm) in case of Ar/4.9%H2-annealed at 1000 measured by tapping mode atomic force microscopy (AFM). The HfON surface was also able to be flattened by reduction of Si surface roughness. The electrical properties of HfON gate insulator were improved by the reduction of Si surface roughness. We obtained equivalent oxide thickness (EOT) of 0.79 nm (as-cleaned: 1.04 nm) and leakage current density of 3.510-3 A/cm2 (as-cleaned: 6.110 -1 A/cm2) by reducing the Si surface roughness.

  • Reduced Surface Roughness of P3HT:PCBM Thin Films with Different Ratios by Electrospray Deposition Methods

    Takeshi FUKUDA  Kenji TAKAGI  Norihiko KAMATA  Jungmyoung JU  Yutaka YAMAGATA  

     
    BRIEF PAPER

      Vol:
    E96-C No:3
      Page(s):
    362-364

    We demonstrated the reduced surface roughness of poly (3-hexylthiophene) (P3HT):(6,6)-phenyl-C61-butyric acid methyl ester (PCBM) thin films with different ratios fabricated by the electrospray deposition (ESD) method. Aggregated structures were observed at the lower voltage, and the uniformity became bad at the higher voltage. Anyway, the minimum root mean square (RMS) roughness was 1.46 nm by optimizing the applied voltage.

  • Experimental Study of Non-specular Wave Scattering from Building Surface Roughness for the Mobile Propagation Modeling

    Hary BUDIARTO  Kenshi HORIHATA  Katsuyuki HANEDA  Jun-ichi TAKADA  

     
    PAPER-Antenna and Propagation

      Vol:
    E87-B No:4
      Page(s):
    958-966

    In the urban area, buildings are the main scatterer which dominate the mobile propagation characteristics. However, reflection, diffraction, and scattering on the building surfaces in the radio environment induce undesirable multipath propagation. Multipath prediction with respect to a building surface has been conventionally based on an assumption that reflection from the surface has a substantial specular direction. However non-specular scattering from the building surface can affect the channel characteristics as well as specular scattering. This paper presents multipath characteristics of non-specular wave scattering from building surface roughness based on the experimental results. Superresolution method was applied as an approach to handle the signal parameters (DoA, ToA) of the individual incoming waves reflected from building surface roughness. The results show that the multipaths can be detected at many scatterers, such as ground, window's glass, window's frames and bricks surface, as well as directly from the transmitter. Most of the scattered waves are arriving closely from specular directions. The measured reflection coefficients were well bounded by reflection coefficients of the theoretically smooth and random rough surface. The Fresnel reflection coefficient formula, considering the finite thickness of the building surface and Gaussian scattering correction, give better prediction for glass and bricks reflection coefficient measurement.

  • Contact Resistance Law for Elasto-Plastic Domains in the Force Range (1 mN-10 N)

    Xavier HERNOT  Abdelhak SENOUCI  Abdelaaziz El MANFALOUTI  Noureddine Ben JEMAA  Rochdi El ABDI  

     
    PAPER-Contact Phenomena

      Vol:
    E86-C No:6
      Page(s):
    874-879

    In this paper, we try to establish a power law for contact resistance versus force Rc = KcFc-n , and we determine via experimental measurements and theoretical calculations, the constants n and Kc in the force range (1 mN-4 N) for bulk metal (Ag, Au, Pd, Ni) used in various applications (microswitches, connectors). The main experimental results of contact resistance are the occurrence of two decrease domains versus progressive load indentation. The first regime corresponds to the earlier touch of the coupon by the probe at force < 0.1 N. This elastic regime evolves to a plastic regime for medium force > 0.1 N. At the transition the exponent value n changes from 0.33 to 0.5 and induce Kc value increasing. Theoretical and computational approaches applied to the elasto-plastic model, confirm the occurrence of these two regimes. Although the calculated values of n are in good agreement with experimental values, some discrepancy between measured and calculated Kc values take place.

  • Estimation of Subsurface Fracture Roughness by Polarimetric Borehole Radar

    Motoyuki SATO  Moriyasu TAKESHITA  

     
    PAPER-Inverse Scattering and Image Reconstruction

      Vol:
    E83-C No:12
      Page(s):
    1881-1888

    Borehole radar is known as a powerful technique for monitoring of subsurface structures such as water flow. However, conventional borehole radar systems are operated in the frequency range lower than 100 MHz and the resolution is poor to measure a surface roughness and an inner structure of subsurface fractures directly. In order to monitor the water flow, these characteristics of subsurface fractures are important. We developed a polarimetric borehole radar system using dipole antennas and axial slot antennas and have found that this system can provide more information than conventional borehole radar. However, the relationship between the characteristic of subsurface fracture and the measured polarimetric radar information has not been clear. In this paper, we simulate electromagnetic wave scattering from subsurface fractures having a rough surface by Finite-Difference Time-Domain (FDTD) technique and discuss the relationship between a surface roughness of subsurface fracture and the polarimetric information. It is found that the subsurface fracture having strong cross-polarized components can be estimated to be rough surface fracture. The full polarimetric single-hole radar measurement was carried out at the Mirror Lake site, NH, USA. In this experiment, we found that subsurface fractures can be classified into some groups by an energy scattering matrix, and found that the subsurface fracture estimated to have a rough surface corresponds to that has higher water permeability.

  • Response of Microwave on Bare Soil Moisture and Surface Roughness by X-Band Scatterometer

    Dharmendra SINGH  Yoshio YAMAGUCHI  Hiroyoshi YAMADA  Keshev Prasad SINGH  

     
    PAPER

      Vol:
    E83-B No:9
      Page(s):
    2038-2043

    This paper describes an individual effect of soil moisture (mg) and surface roughness (hrms) of bare soil on the back scattering coefficient (σ0) at the X-band frequency. The study contributes to the design of an efficient microwave sensor. For this purpose, experimentally observed data was utilized to provide a composite σ0 equation model accounting for individual effect in regression analysis. The experimental data are compared with Small Perturbation Method. It is observed that the X-band gives better agreement up to incidence angle 50 for HH-polarization and 60 for VV-polarization as compared to the C-band. The lower angles of incidence give better results than the higher angles for observing mg at the X-band. The multiple and partial regression analyses have also carried out for predicting the dependence of scattering coefficient (σ0) on mg and hrms more accurately. The analyses suggest that the dependence of dielectric constant (i.e., mg) is much more significant in comparison to surface roughness at lower angles of incidence for both like polarizations. The results propose the suitable angle of incidence for observing bare surface roughness and soil moisture at the X-band. All these data can be used as a reference for satellite or spaceborne sensors.

  • Micro Recording Performance Fluctuation and Magnetic Roughness Analysis: Methodology and Application

    Bo LIU  Wei ZHANG  Sheng-Bin HU  

     
    PAPER

      Vol:
    E83-C No:9
      Page(s):
    1530-1538

    As technology moves at an annual area density increase rate of 80-120% and channel density moves beyond 3, micro-fluctuation of media recording performance and the homogeneity of media's recording capability become serious reliability concerns in future high density magnetic recording systems. Two concepts are proposed in this work for the characterization of the micro-recording performance fluctuation at high bit and channel densities: recording performance roughness analysis and dynamic magnetic roughness analysis. The recording performance roughness analysis is based on an in-situ measurement technique of the non-linear transition shift (NLTS). Relationship between the performance roughness and the roughness of dynamic magnetic parameters are studied. Results of experimental investigations indicate that the NLTS based performance roughness analysis can reveal more details on media's recording capability and the capability fluctuation--the macro and micro fluctuation of recording performance. The dynamic magnetic roughness analysis is read/write operation based and can be used to characterize the macro and micro fluctuation of media's dynamic magnetic properties. The parameters used for the analysis include media's dynamic coercivity and the dynamic coercive squareness. Here, "dynamic" refers to the dynamic performance measured at MHz frequency. The authors also noticed in their technology development process that further methodology development and confirmation are necessary for media's dynamic performance analysis. Therefore, the work also extends to the accuracy analysis of the playback amplitude based methods for the analysis of the dynamic coercive squareness and dynamic hysteresis loop. A method which is of smaller testing error is identified and reported in this work.

  • In Situ Fiber Optical Sensor for the Measurement of Thin Films

    Yifei HE  Brian W. SHELDON  Theodore F. MORSE  

     
    PAPER-Physical and Mechanical Sensors

      Vol:
    E83-C No:3
      Page(s):
    315-325

    A novel technique has been developed for in situ sensing of thin film growth. In this method, a fiber optic probe is placed at an appropriate position in a deposition chamber, and the thin film builds up on the end of the fiber. This film is either the same as on the wafer where deposition occurs, or it bears a fixed relationship to the film on the wafer. By an analysis of the intensity of the light reflected from the film and guided by the fiber, information on the film may be obtained. With interference causing maxima, minima and a point of inflection as the film grows, it is possible to obtain near real time information on the following quantities: the real and imaginary parts of the refractive index of the film, a Gaussian parameter characterizing surface roughness, and the film thickness itself. To demonstrate this technique, we have studied the deposition of silicon nitride films in a CVD reactor and how reactor temperature and reactant flow rates influence film growth. This technique may be applied to measure in situ reflectivity of multi layer films, so that reflectance as a function of temperature and time may be obtained. Because the measurement is simple and direct and the information is optical, we believe that this technique has the potential to supplant quartz oscillators in the measurement of thin film growth.

  • Probability Model and Its Application on the Interaction of Nano-Spaced Slider/Disk Interface

    Wei HUA  Bo LIU  Gang SHENG  

     
    PAPER

      Vol:
    E82-C No:12
      Page(s):
    2139-2147

    The effect of surface roughness is crucial for contact recording and proximity recording. In this paper a probability model is developed for investigation of the influence of surface roughness on flying performance and the contact force of the slider. Simulations are conducted for both the contact recording slider and the proximity recording slider, and the results are well coordinated with the reported experimental results and the self-conducted experimental results. Studies are further extended to the characterization of the roughness of the air bearing surface and the disk surface that may support head/disk spacing between 5 nm and 15 nm.

  • Evaluation of Arachidic Acid Langmuir-Blodgett Ultrathin Films on Silver Thin Films from Scattered Light Using Surface Plasmon Polariton Excited at the Interfaces

    Yusuke AOKI  Keizo KATO  Kazunari SHINBO  Futao KANEKO  Takashi WAKAMATSU  

     
    PAPER

      Vol:
    E81-C No:7
      Page(s):
    1098-1105

    Attenuated total reflection (ATR) properties and scattered light properties were measured for Ag thin films and arachidic acid (C20) Langmuir-Blodgett (LB) ultrathin films on the Ag thin films to obtain the information about their complex dielectric constants and surface roughness utilizing an excited surface plasmon polariton. The complex dielectric constants for the Ag thin films and the C20 LB films were obtained by fitting the calculated ATR curves to the experimental ones. The surface roughnesses of these films were estimated by the angular distribution of the scattered light assuming the Gaussian function as an autocorrelation function and a linear superposition of roughness spectra. The angular spectra strongly depended on the roughness parameters: the transverse correlation length σ and the surface corrugation depth δ. The experimental angular distributions were explained by some pairs of σ and δ. It was suggested that the surface roughness of the C20 LB films changed with the number of monolayers since the angular spectra varied with the number of the C20 LB monolayers on the Ag films. It is thought that the measurement of the scattered light is useful to evaluate surface roughnesses of LB ultrathin films.

  • A Proposal on Contact Surface Model of Electromagnetic Relays Based on the Change in Showering Arc Waveforms with the Number of Contact Operations

    Kiyotomi MIYAJIMA  Shuichi NITTA  Atsuo MUTOH  

     
    PAPER

      Vol:
    E81-C No:3
      Page(s):
    399-407

    The showering arc waveforms generated when contact is being separate have poor reproducibility whose causes are not sufficiently clear. This paper describes that the contact surface conditions which change with the number of contact operations are deeply related to the showering arc waveforms. First, it is experimentally shown that the contacts' surface roughness increases with the number of contact operations, and the growth model of contact surface roughness is proposed based on the change of contact resistance for the number of contact operations. Second, the growth model of molten metal bridge is proposed based on the fact that the showering arc waveforms change with the number of contact operations and the evaluation indexes of showering arc are proposed.

  • AFM Characterization of GaAs/AlGaAs Waveguides

    Kazuhiko HOSOMI  Masataka SHIRAI  Kenji HIRUMA  Junji SHIGETA  Toshio KATSUYAMA  

     
    PAPER

      Vol:
    E79-C No:11
      Page(s):
    1579-1585

    The direct measurement of sidewall roughness on a ridge-type GaAs waveguide was performed using an atomic force microscope (AFM) combined with a scanning electron microscope (SEM). The ridge sidewall of a GaAs waveguide formed by wet-etching and the ridge sidewall formed after regrowth of a 2.45-µm GaAs/AlGaAs epitaxial layer on the same waveguide were observed using introducing the technique for sample slanting. The observed power spectral density was used to determine the scattering loss caused by the sidewall roughness. It was found that the ridge-type GaAs waveguide for light wave transmission had a scattering loss of 0.029 dB/cm in the as-etched ridge state and a scattering loss of 0.17 dB/cm after regrowing the cover GaAs/AlGaAs epitaxial layer. A leaky GaAs/AlGaAs waveguide for polariton-quantum-wave trans-mission had a scattering loss of 1.3l0-5 dB/cm, which means that the scattering loss is negligible. Furthermore, it was found that a periodical surface fluctuation (spatial frequency 2.2 µm-1) along the waveguide appeared after the regrowth of the epitaxial layer. Thus, this method is useful for direct observation of sidewall roughness and can be used to quantitatively determine the sidewall scattering loss.

  • Self-Holding Optical Switch Using Optical Matrix Board

    Shuichiro INAGAKI  Yoriko HANAOKA  Tsuneo KANAI  

     
    PAPER-Connectors: Optical and Conventional

      Vol:
    E77-C No:10
      Page(s):
    1553-1558

    A new self-holding optical switch that consists of an optical matrix board and a precision robot is proposed. Fabrication and evaluation of 33 optical matrix boards confirm the feasibility of large-size optical switching. Suppressing deviations in the groove position will realize lower loss optical matrix boards in the near future. The apparent roughness of the groove walls can be evaluated simply and effectively by measuring return loss with an interferometric optical-time-domain reflectometer.

  • Effects of Cleaning by Sulfuric Acid and Hydroperoxide Mixture on Thin SiO2 Film Properties

    Masashi MAEKAWA  Shigeo OHNISHI  Keizo SAKIYAMA  

     
    PAPER

      Vol:
    E75-C No:7
      Page(s):
    796-799

    Effects of cleaning by H2SO4: H2O2 on thin SiO2 film was investigated. The cleaning increases Fowler-Nordheim currents by about 14%, shifts the dielectric breakdown distribution to lower electric field intensity and degrades TDDB characteristics. These results are due to the oxidation and commensurate roughening of the silicon srface by the cleaning solution. When the cleaning is done at higher temperature and with higher concentration of hydroperoxide, microroughness of silicon surface increases. Therfore, the trade-off between the cleaning effect and the roughening effect of H2SO4: H2O2 should be found out.

  • Influence of Vacancy in Silicon Wafer of Various Types on Surface Microroughness in Wet Chemical Process

    Tadahiro OHMI  Toshihito TSUGA  Jun TAKANO  Masahiko KOGURE  Koji MAKIHARA  Takayuki IMAOKA  

     
    PAPER

      Vol:
    E75-C No:7
      Page(s):
    800-808

    The increase of surface microroughness on Si substrate degrades the electrical characteristics such as the dielectric breakdown field intensity (EBD) and charge to break-down (QBD) of thin oxide film. It has been found that the surface microroughness increases in the wet chemical process, particularly in NH4OH-H2O2-H2O cleaning (APM cleaning). It has been revealed that the surface microroughness does not increase at all if the NH4OH mixing ratio in NH4OH-H2O2-H2O solution is reduced from the conventional level of 1:1:5 to 0.05:1:5, and the room temperature ultrapure water rinsing is introduced right after the APM cleaning. At the same time, the APM cleaning with NH4OH-H2O2-H2O mixing ratio of 0.05:1:5 has been very effective to remove particles and metallic impurities from the Si surface. The surface microroughness dominating the electrical properties of very thin oxide films is strictly influenced by the wafer quality. The increase of surface microroughness due to the APM cleaning has varied among the wafer types such as Cz, FZ and epitaxial (EPI) wafers. The increase of surface microroughness in EPI wafer was very much limited, while the surface microroughness of FZ and Cz wafers gradually increase. As a result of investigating the amount of diffused phosphorus atoms into these wafers, the increase of the surface microroughness in APM cleaning has been confirmed to strongly depend on the silicon vacancy cluster concentration in wafer. The EPI wafer having low silicon vacancy concentration is essentially revealed superior for future sub-half-micron ULSI devices.

  • Evaluation of Si Surface Micro-Roughness by Measuring Chlorine Concentration and Total Charge of Native Oxide

    Ichiro OKI  Tetsuo BIWA  Jun KUDO  Hikou SHIBAYAMA  

     
    PAPER

      Vol:
    E75-C No:7
      Page(s):
    809-811

    We have developed a new method of evaluating Si suface micro-roughness, by forming thin oxide in HCl/H2O2 solution and then measuring the concentration of chlorine atomes and the total charge in this oxide. It is shown that this oxide does not affect the surface micro-roughness, and the surface concentration of chlorine atoms incorporated in this oxide and the total oxide charge are proportional to the surface microroughness, obtained by AFM. From this correlation, it is possible to evaluate the surface micro-roughness for large areas compared with the areas of AFM measurement.